Method for mixing fluids

Patent metadata

Field	Value
Publication number	US-10022690-B2
Application number	US-201514737137-A
Country	US
Kind code	B2
Filing date	Jun 11, 2015
Priority date	Jun 11, 2014
Publication date	Jul 17, 2018
Grant date	Jul 17, 2018

Abstract

A method and apparatus for mixing at least two fluids is provided. The method involves using means for providing a spiral stream of a first fluid and a second fluid is injected directly inside the first fluid to achieve effective mixing.

First claim

What is claimed is:

1. A method of mixing fluids in a fluid mixer, the fluid mixer comprising a first inlet, a second inlet, an outlet, and a substantially cylindrical mixing chamber, the mixing chamber comprising a wall, a top plate, and a bottom plate, and the method comprising:
passing a first fluid stream into the mixing chamber through the first inlet, the first inlet having openings in the top plate and inside the mixing chamber, an outer wall of the first inlet extending to the wall of the mixing chamber and descending to the bottom of the mixing chamber;
providing a spiral stream of the first fluid inside the mixing chamber through the first inlet, the first inlet descending to the mixing chamber in the form of a ramp or a pipe, and forming an asymmetry to the cylindrical shape to enhance spiral stream in the mixing chamber;
injecting through the second inlet, and tangential to the wall of the mixing chamber, a second fluid into the spiral stream of the first fluid such that the concentration of the second fluid decreases towards the wall of the mixing chamber; and
directing the spiral stream of the fluids to the exterior of the mixing chamber as a vortex through the outlet, the outlet being provided in the bottom plate, and the outlet being concentric with the spiral flow axis.

2. The method as claimed in claim 1 , wherein the first inlet has a height corresponding to the height of the mixing chamber.

3. The method as claimed in claim 1 , wherein the second inlet includes a nozzle with an inner sleeve for protecting the second inlet from corrosion.

4. The method as claimed in claim 1 , wherein the second fluid includes an agent which is corrosive.

5. The method as claimed in claim 1 , wherein the volume ratio of the first fluid to the second fluid in the fluid stream exiting the mixing chamber is from 1:1 to 15:1.

6. The method as claimed in claim 1 , wherein the second fluid comprises:
one or more free fatty acid distillates,
one or more free fatty acid containing bio based feedstock,
by-products from fatty acid methyl ester and bio based chemicals production and/or oil derived from ligno-cellulosic biomass, and/or
one or more lower molecular weight acids containing bio based feedstock.

7. The method as claimed in claim 1 , wherein the flow rate of the first fluid is higher than the flow rate of the second fluid.

8. The method as claimed in claim 1 , wherein the flow inside the mixing chamber is controlled by injecting the second fluid into and concurrent to the first fluid such that the second fluid does not touch the wall of the mixing chamber.

9. The method as claimed in claim 1 , wherein the spiral flow rotates from 0.5 to 2 r/s inside the mixing chamber.

10. The method as claimed in claim 1 , wherein the first fluid is fed 50-300 t/h and the second fluid is fed 0.5-20 t/h.

11. The method as claimed in claim 1 , wherein the height of the mixing chamber is smaller than its diameter.

12. The method as claimed in claim 1 , wherein the mixing of fluid is extended inside a downflow reactor or a reactor comprising multiple beds.

13. The method as claimed in claim 1 , wherein the second fluid contains free fatty acid containing renewable hydrocarbon source of biological origin and the first fluid contains incoming process feed.

14. The method as claimed in claim 1 , wherein the second fluid includes up to 100% w/w free fatty acid.

15. The method as claimed in claim 1 , wherein the method is conducted using a fluid mixer comprising:
a substantially cylindrical mixing chamber being defined by a wall, a top plate, and a bottom plate;
a first inlet for passing a first fluid stream into the mixing chamber, the first inlet having openings in the top plate and inside the mixing chamber, an outer wall of the first inlet extending to the wall of the mixing chamber and descending to the bottom of the mixing chamber, the first inlet being configured to provide a spiral stream of the first fluid inside the mixing chamber, the first inlet descending to the mixing chamber in the form of a ramp or a pipe, and forming an asymmetry to the cylindrical shape to enhance spiral stream in the mixing chamber;
a second inlet for injecting tangentially to the wall of the mixing chamber a second fluid into the spiral stream of the first fluid such that the concentration of the second fluid decreases towards the wall of the mixing chamber, the second inlet optionally comprising a nozzle with an inner sleeve for protecting the second inlet from corrosion; and
an outlet in the bottom plate, the fluid mixer being configured to direct the spiral stream of the fluids to the exterior of the mixing chamber as a vortex through the outlet, the outlet being concentric with the spiral flow axis.

16. The method as claimed in claim 1 , wherein the volume ratio of the first fluid to the second fluid in the fluid stream exiting the mixing chamber is from 3:1 to 6:1.

17. The method as claimed in claim 1 , wherein the second fluid comprises:
palm fatty acid distillate and/or soya free fatty acid distillate,
crude and refined palm based oil, technical corn oil, tall oil, seed oil, animal fat, waste cooking oil, jatropha curcas oil, fish oil, microbial oil, and/or algae oil, and/or
pyrolysis oil and/or sludge palm oil.

18. The method as claimed in claim 1 , wherein the height of the mixing chamber is smaller than its diameter, wherein the height to diameter ratio is from 0.03 to 0.15.

19. The method as claimed in claim 1 , wherein the second fluid includes up to 95% w/w free fatty acid.

20. A fluid mixer comprising:
a substantially cylindrical mixing chamber being defined by a wall, a top plate, and a bottom plate;
a first inlet for passing a first fluid stream into the mixing chamber, the first inlet having openings in the top plate and inside the mixing chamber, an outer wall of the first inlet extending to the wall of the mixing chamber and descending to the bottom of the mixing chamber, the first inlet being configured to provide a spiral stream of the first fluid inside the mixing chamber, the first inlet descending to the mixing chamber in the form of a ramp or a pipe, and forming an asymmetry to the cylindrical shape to enhance spiral stream in the mixing chamber;
a second inlet for injecting tangentially to the wall of the mixing chamber a second fluid into the spiral stream of the first fluid such that the concentration of the second fluid decreases towards the wall of the mixing chamber, the second inlet optionally comprising a nozzle with an inner sleeve for protecting the second inlet from corrosion; and
an outlet in the bottom plate, the fluid mixer being configured to direct the spiral stream of the fluids to the exterior of the mixing chamber as a vortex through the outlet, the outlet being concentric with the spiral flow axis.

21. The fluid mixer as claimed in claim 1 , wherein
the second inlet is directed downstream and separated from the wall of the mixing chamber; and/or
the outlet is circular and has a diameter smaller than the diameter of the mixing chamber.

Assignees

• Neste Oyj

Inventors

• Riska Anders
• Joona Sumela
• Vaittinen Johanna

Classifications

• B01J19/2405

  provoking a turbulent flow of the reactants, such as in cyclones, or having a high Reynolds-number · CPC title

• B01J14/00 Primary

  Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor (B01J8/00, B01J19/08 take precedence) · CPC title

• B01J4/00

  Feed {or outlet} devices; Feed or outlet control devices (feed or outlet devices for pressure vessels B01J3/02 {; feeding of particles into and evacuation of particles out of the reactor B01J8/0015}) · CPC title

• B01J2219/00164

  controlling the flow · CPC title

• B01J2204/007

  Aspects relating to the heat-exchange of the feed or outlet devices · CPC title