Micro-interface enhanced oxidation system and oxidation method for preparing hydrogen peroxide
US-12090458-B2 · Sep 17, 2024 · US
US10016736B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10016736-B2 |
| Application number | US-201415032401-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 22, 2014 |
| Priority date | Oct 29, 2013 |
| Publication date | Jul 10, 2018 |
| Grant date | Jul 10, 2018 |
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A cyclonic reactor vessel comprising: a primary cyclonic separation device disposed within the shell and having an outlet; a plurality of secondary cyclones, said secondary cyclones being disposed within the shell, and each of said secondary cyclones having a body, an inlet and an outlet; wherein the outlet of the primary cyclonic separation device is connected to the inlet of at least one secondary cyclone; a first plenum having a skirt and a floor forming a sealed annular chamber within the shell; a second plenum having a smaller volume than a volume of the first plenum; and a secondary cyclone support system minimizing or eliminating mechanical thermal stresses; and wherein the outlets of the plurality of secondary cyclones are fluidly connected to the second plenum is provided.
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We claim: 1. A cyclonic reactor vessel comprising: a shell; a primary cyclonic separation device disposed within the shell and having an outlet; a plurality of secondary cyclones, said secondary cyclones being disposed within the shell, and each of said secondary cyclones having a body, an inlet and an outlet; wherein the outlet of the primary cyclonic separation device is connected to the inlet of at least one secondary cyclone such that a fluid stream may flow from the outlet of the primary cyclonic separation device into the inlet of the at least one secondary cyclone; a first plenum having a skirt and a floor forming a sealed annular chamber within the shell, wherein the first plenum is supported within the shell by attachment to the shell; a second plenum having an outlet tube for removing gasses from within the shell, a skirt and a floor and having a smaller volume than a volume of the first plenum; and a secondary cyclone support system comprising at least one mechanism selected from the group consisting of: (a) attachment of the outlet tube of each secondary cyclone to the skirt and/or floor of the first plenum and (b) a first set of hanger straps extending from the first plenum skirt and/or first plenum floor and/or secondary cyclone outlet pipe to the body of each secondary cyclone, wherein the first set of hanger straps are substantially vertically placed within the shell; and wherein the outlets of the plurality of secondary cyclones are fluidly connected to the second plenum. 2. The cyclonic reactor vessel according to claim 1 , wherein the secondary cyclone support system minimizes mechanical thermal stresses between the first and second plenums and the secondary cyclones. 3. The vessel according to claim 1 , wherein the primary cyclonic separation device comprises at least one primary cyclone, each primary cyclone having an inlet and an outlet. 4. The vessel according to claim 3 , wherein each primary cyclone is attached to the skirt and/or floor of the first plenum by way of a second set of hanger straps and wherein the second set of hanger straps are substantially vertically. 5. The vessel according to claim 1 , wherein the outlets of the secondary cyclones are connected to the second plenum by way of a sliding fit. 6. The vessel according to claim 1 , wherein the first plenum further comprises a purge gas inlet. 7. The vessel according to claim 1 , wherein the vessel is selected from the group consisting of fluidized bed reactors, riser reactors, fast fluidized reactors, turbulent bed reactors, fluidized catalytic cracking reactors, fluidized catalytic cracking regenerators and gassifiers. 8. The vessel according to claim 1 , wherein the residence time of a gas in the second plenum is less than or equal to 0.4 seconds. 9. The vessel according to claim 7 , wherein the second plenum is configured to dehydrogenate propane and a propylene selectively penalty from the entry to the outlet of the second plenum is equal to or less than 0.4 mole %.
Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction (B01J8/0285, B01J8/067, B01J8/087, B01J8/1836 take precedence) · CPC title
using cyclones · CPC title
Accessories, e.g. safety or control devices, not otherwise provided for {, e.g. regulators, valves in inlet or overflow ducting}(with electrostatic precipitating arrangements B03C3/14) · CPC title
controlling the residence time inside the reactor vessel · CPC title
Apparatus for generating gases (production of inert gas mixtures B01J19/14; for generating specific gases, see the relevant subclasses, e.g. C01B, C10J {; in "air bags" on vehicles B60R21/26; for starter gas F02C7/26; blasting cartridges for producing gas under pressure F42B3/04}) · CPC title
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