Method for heating a slurry system

Patent metadata

Field	Value
Publication number	US-10010938-B2
Application number	US-201414520129-A
Country	US
Kind code	B2
Filing date	Oct 21, 2014
Priority date	Oct 22, 2013
Publication date	Jul 3, 2018
Grant date	Jul 3, 2018

Abstract

A reservoir for one or more chemical reactants has means for heating the reactants and optional means for stirring the reactants. A pumped reactant feed line and a return line provide fluid communication between the reservoir and a 4-way valve system. The 4-way valve system is also in fluid communication with a reactor vessel and a source of inert gas for purging the system. In a first state, the 4-way valve provides fluid communication between the reservoir and the reactor. In a second state, the 4-way valve provides a continuous circulation path for the heated reactants from the reservoir, to the valve system, and back to the reservoir via the return line. In a third state, the 4-way valve provides a fluid pathway for purging the reactor with inert gas. In a fourth state, the 4-way valve provides a fluid pathway for purging the reservoir with inert gas.

First claim

What is claimed is:

1. An apparatus comprising:
a reactor;
a reservoir;
a heater in thermal contact with the reservoir;
a pump;
a valve assembly having a first 3-port valve and a second 3-port valve;
a first transparent supply line in fluid communication with the reservoir at a first end thereof and with the pump at a second end thereof;
a second transparent supply line in fluid communication with the pump at a first end thereof and with the valve assembly at a second end thereof;
a delivery line in fluid communication with the valve assembly at a first end thereof and with the reactor at a second end thereof;
a transparent return line in fluid communication with the valve assembly at a first end thereof and with the reservoir at a second end thereof;

wherein the valve assembly is configured such that in a first state the valve assembly provides fluid communication from the reservoir to the reactor via the first supply line, the pump, the second supply line, and the delivery line and, in a second state, provides recirculation of the contents of the reservoir via the first supply line, the pump, the second supply line, and the return line.

2. The apparatus recited in claim 1 further comprising:
a source of inert gas;
a purge line in fluid communication with the source of inert gas at a first end thereof and with the valve assembly at a second end thereof;

wherein the valve assembly is configured such that in a third state the valve assembly provides fluid communication between the source of inert gas and the reactor via the purge line and the delivery line.

3. The apparatus recited in claim 2 further wherein the valve assembly is configured such that in a fourth state the valve assembly provides fluid communication between the source of inert gas and the reservoir via the purge line and the return line.

4. The apparatus recited in claim 1 wherein the first supply line is contiguous with the second supply line and the pump is a peristaltic pump.

5. The apparatus recited in claim 1 further comprising means for stirring the contents of the reservoir.

6. The apparatus recited in claim 5 wherein the means for stirring the contents of the reservoir is a magnetic stirrer.

7. The apparatus recited in claim 6 wherein the magnetic stirrer is housed within the heater.

8. The apparatus recited in claim 1 wherein a common port of the first 3-port valve is in fluid communication with a common port of the second 3-port valve.

9. The apparatus recited in claim 1 further comprising:
a scale configured to weigh the contents of the reservoir.

10. The apparatus recited in claim 1 further comprising:
a timer configured to control the pump and the valve assembly.

11. The apparatus recited in claim 1 further comprising:
a timer configured to control the pump, the valve assembly, and the heater.

12. The apparatus recited in claim 11 further comprising:
means for stirring the contents of the reservoir; and,

wherein the timer is configured to additionally control the means for stirring the contents of the reservoir.

13. The apparatus recited in claim 1 wherein the delivery line is transparent.

14. An apparatus comprising:
a reactor;
a reservoir;
a heater in thermal contact with the reservoir;
a pump;
a valve assembly having a first 3-port valve and a second 3-port valve;
a first transparent supply line in fluid communication with the reservoir at a first end thereof and with the pump at a second end thereof;
a second transparent supply line in fluid communication with the pump at a first end thereof and with the valve assembly at a second end thereof;
a delivery line in fluid communication with the valve assembly at a first end thereof and with the reactor at a second end thereof;
a transparent return line in fluid communication with the valve assembly at a first end thereof and with the reservoir at a second end thereof;
at least one temperature sensor in thermal contact with at least one of the reactor, the first supply line, the second supply line, the valve assembly, and the return line;
a processor-based system in data communication with the at least one temperature sensor and configured to control the heater, the pump, and the valve assembly;

wherein the valve assembly is configured such that in a first state the valve assembly provides fluid communication from the reservoir to the reactor via the first supply line, the pump, the second supply line, and the delivery line and, in a second state, provides recirculation of the contents of the reservoir via the first supply line, the pump, the second supply line, and the return line.

15. The apparatus recited in claim 14 further comprising a medium storing instructions for causing the processor-based system to:
position the valve assembly in the second state; and,
actuate the heater and the pump so as to maintain a preselected minimum temperature in at least one of the group consisting of the first supply line, the second supply line and the return line.

16. The apparatus recited in claim 14 further comprising a scale in data communication with the processor-based system and configured to weigh the contents of the reservoir.

17. The apparatus recited in claim 16 further comprising a medium storing instructions for causing the processor-based system to:
position the valve assembly in the first state; and,
actuate the pump so as to supply a preselected quantity by weight of the contents of the reservoir to the reactor.

18. The apparatus recited in claim 14 further comprising:
a heat exchanger in fluid communication with the first transparent supply line.

19. A method for maintaining a slurry of reactants in a fluid state comprising:
providing:
a reactor;
a reservoir contain a slurry of reactants;
a heater in thermal contact with the reservoir;
a pump;
a valve assembly having a first 3-port valve and a second 3-port valve;
a first transparent supply line in fluid communication with the reservoir at a first end thereof and with the pump at a second end thereof;
a second transparent supply line in fluid communication with the pump at a first end thereof and with the valve assembly at a second end thereof;
a delivery line in fluid communication with the valve assembly at a first end thereof and with the reactor at a second end thereof;
a transparent return line in fluid communication with the valve assembly at a first end thereof and with the reservoir at a second end thereof;

wherein the valve assembly is configured such that in a first state the valve assembly provides fluid communication from the reservoir to the reactor via the first supply line, the pump, the second supply line, and the delivery line and, in a second state, provides recirculation of the contents of the reservoir via the first supply line, the pump, the second supply line, and the return line;
visually monitoring the slurry of reactants in the first transparent supply line, the second transparent supply line and the transparent return line;
positioning the valve assembly into the second state; and,
actuating the heater and the pump to recirculate the heated slurry of reactants from the reservoir through the first supply line, the pump, the second supply line, the valve assembly, and the return line back to the reservoir.

20. An apparatus comprising:
a reactor;
a reservoir;
a heater in thermal contact with the reservoir;
a pump;
a valve assembly;
a source of inert gas;
a purge line in fluid commun

Assignees

• Nanoco Technologies Ltd

Inventors

• Boag Neil
• Gooda Andrew

Classifications

• B01J2219/0011

  involving reactant liquids · CPC title

• B01J2219/00231

  at the reactor inlet · CPC title

• B01J2208/00539

  Pressure · CPC title

• B01J2219/00063

  of the reactants · CPC title

• B01J2219/00069

  Flow rate measurement · CPC title