Methods and apparatuses for measuring material phase properties

Patent metadata

Field	Value
Publication number	US-10001435-B1
Application number	US-201715482000-A
Country	US
Kind code	B1
Filing date	Apr 7, 2017
Priority date	Apr 7, 2017
Publication date	Jun 19, 2018
Grant date	Jun 19, 2018

Abstract

Methods and apparatuses for determining a material characteristic of a sample material are disclosed. A sample material is loaded to a plurality of cells. An interference material is disposed relative to the sample material such that the interference material at least retards the transport of the sample material from a one of the cells to at least another one of the cells. For each one of the cells, independently: a stimulus is applied to the sample material in the cell such that a conditioned sample material is obtained; and a material characteristic of the conditioned sample material is sensed.

First claim

What is claimed is:

1. A method for determining a material characteristic of a sample material comprising:
loading a sample material to a plurality of cells;
disposing an interference material relative to the sample material such that the interference material at least retards the transport of the sample material from a one of the cells to at least another one of the cells; and
for each one of the cells, independently:
applying a stimulus to the sample material in the cell such that a conditioned sample material is obtained; and
sensing a material characteristic of the conditioned sample material.

2. The method of claim 1 , wherein the applying the stimulus modulates pressure, temperature, voltage, radiation dose, electric field, magnetic field, or a combination thereof of the sample material in the cell.

3. The method of claim 2 , wherein the applying the stimulus modulates the pressure of the sample material in the cell.

4. The method of claim 2 , wherein the applying the stimulus comprises pressurizing the interference material, wherein the interference material communicates pressure to the cell thereby modulating the pressure of the sample material in the cell.

5. The method of claim 2 , wherein the applying the stimulus modulates temperature of the sample material in the cell.

6. The method of claim 5 , wherein the temperature is modulated by a heat exchanger.

7. The method of claim 6 , wherein at least a portion of the heat exchanger is integral with at least a portion of the cell.

8. The method of claim 2 , wherein the plurality of cells comprises a plurality of rows and a plurality of columns, the stimulus modulates a first material property selected from pressure, temperature, voltage, radiation dose, electric field, and magnetic field parameter such that the first material property is substantially constant in cells of a row of the plurality of rows, and wherein the stimulus modulates a second material property selected from pressure, temperature, voltage, radiation dose, electric field, and magnetic field parameter such that the second material property is substantially constant in cells of a column of the plurality of columns.

9. The method of claim 1 , wherein the transport being retarded includes transport across an interface between the sample material and the interference material.

10. The method of claim 1 , further comprising determining a critical point, a dew point, a bubble point, a melting point, a boiling point, a eutectic point, a cricondentherm, a cricondenbar, quality lines, or a combination thereof using the sensed material characteristic.

11. A method for determining a material characteristic of a material comprising:
flowing a material through a main channel such that a first pressure is established and is communicated to a branch channel from the main channel;
applying a first stimulus to material within a first space of the branch channel for modulating a material property parameter of the material within the first space of the branch channel;
applying a second stimulus to material within a second space of the branch channel for modulating a material property parameter of the material within the second space of the branch channel;
sensing a material characteristic of the material within the first space of the branch channel; and
sensing a material characteristic of the material within the second space of the branch channel.

12. The method of claim 11 , wherein the material property parameter of the material within the first space of the branch channel, and the material property parameter of the material within the second space of the branch channel are, independently, temperature.

13. The method of claim 11 , wherein the flowing of the material through the main channel establishes a second pressure downstream from the first pressure, and wherein the second pressure is communicated to a downstream branch channel, the downstream branch channel connecting to the main channel downstream of the branch channel;
wherein the method further comprises:
applying a third stimulus to material within a first space of the downstream branch channel for modulating a material property parameter of the material within the first space of the downstream branch channel;
applying a fourth stimulus to material within a second space of the downstream branch channel for modulating a material property parameter of the material within the second space of the downstream branch channel;
sensing a material characteristic of the material within the first space of the downstream branch channel; and
sensing a material characteristic of the material within the second space of the downstream branch channel.

14. The method of claim 13 , wherein the branch channel and the downstream branch channel are substantially parallel, wherein the distance from the connection point of the main channel and the branch channel to the first space of the branch channel is about equal to the distance from the connection point of the main channel and the downstream branch channel to the first space of the downstream branch channel, and wherein the modulated material property of the material within the first space of the branch channel is modulated to a substantially equal condition to the modulated material property of the material within the first space of the downstream branch channel.

15. The method of claim 11 , wherein the branch channel comprises a first cell and a second cell, the first space of the branch channel being defined by the first cell, the second space of the branch channel being defined by the second cell,
wherein the material within the first space of the branch channel is a first sample fluid, and the material within the second space of the branch channel is a second sample fluid; and
wherein the flowed material is an interference material that at least retards the transport of the first sample fluid from the first space of the branch channel to the second space of the branch channel, and at least retards the transport of the second sample fluid from the second space of the branch channel to the first space of the branch channel.

16. An apparatus for determining phase properties of a sample material comprising:
a fluid device comprising:
a plurality of cells;
a channel connected to the plurality of cells, the channel configured receive a flow of an interference material such that the interference material at least retards the transport of a sample material disposed one of the cells to another of the cells;

a stimulator configured to apply an individual stimulus to each one of the cells to condition sample material disposed therein; and
a sensor configured to sense a material characteristic of material within each one of the cells.

17. The apparatus of claim 16 , wherein the stimulator comprises a pressure modulator for modulating the pressure of material within each one of the cells.

18. The apparatus of claim 16 , wherein the channel comprises a main channel and at least one branch channel connected to the main channel configured such that, when the interference material is pumped through the main channel, the pressure in each branch channel, independently, is substantially the same.

19. The apparatus of claim 16 , wherein the device comprises an sensory layer and an etched layer, wherein the volumes of the channel and the volumes of the plurality of walls are defined by void space between the sensory layer and the etched layer.

20. The apparatus of claim 16 , wherein the stimulator comprises a te

Assignees

• Governing Council Univ Toronto

Inventors

• Sinton David
• Riordon Jason
• Xu Yi
• Bao Bo

Classifications

• G01N1/4022

  by thermal techniques; Phase changes · CPC title

• B01L3/50273 Primary

  characterised by the means or forces applied to move the fluids · CPC title

• G01R33/12

  Measuring magnetic properties of articles or specimens of solids or fluids (involving magnetic resonance G01R33/20) · CPC title

• B01L2400/0487

  fluid pressure, pneumatics · CPC title

• B01L2300/14

  Means for pressure control · CPC title